Download Analytical Calorimetry: Proceedings of the American Chemical by J. F. Jackson, L. Mandelkern (auth.), Roger S. Porter, PDF

By J. F. Jackson, L. Mandelkern (auth.), Roger S. Porter, Julian F. Johnson (eds.)

ISBN-10: 1475700032

ISBN-13: 9781475700039

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Additional resources for Analytical Calorimetry: Proceedings of the American Chemical Society Symposium on Analytical Calorimetry, San Francisco, California, April 2–5, 1968

Sample text

And p-toluic acid of high 45 J. R. KNOX 46 Figure 1. 8 T, ti c! POLYPROPYLENE ~ l 2000C. To= 126°C. ) Figure 2. 9 POLYPROPYLENE Tf T. 6 ! 1 o o Figure 3. R. 9 / / Figure 4. KNOX 48 purity and known heat of fusion. 147 in 2 /sec. was obtained from the data on all of the standards. 9 ca1/g. As the crystallization temperature increases, the percent crystallinity which is developed at that temperature decreases. For this reason it was decided to compare rates of crystallinity development on a reduced crystallinity basis.

KNOX 46 Figure 1. 8 T, ti c! POLYPROPYLENE ~ l 2000C. To= 126°C. ) Figure 2. 9 POLYPROPYLENE Tf T. 6 ! 1 o o Figure 3. R. 9 / / Figure 4. KNOX 48 purity and known heat of fusion. 147 in 2 /sec. was obtained from the data on all of the standards. 9 ca1/g. As the crystallization temperature increases, the percent crystallinity which is developed at that temperature decreases. For this reason it was decided to compare rates of crystallinity development on a reduced crystallinity basis. The reduced crystallinity was calculated as the amount of crystallinity developed at any time divided by the total crystallinity attained at that tel"lperature.

Samples weighing about 5 mg were contained in covered aluminum sample pans. Areas of the exotherms were 41 42 R. W. FORD, J. D. ILAVSKY, AND R. A. SCOTT measured with a planimeter. Heats of melting and melting points were determined on both annealed samples and samples which were subjected to various prior thermal histories. , then cool to 75°C at 10°C/min. Melting points were run at 5°C/min. Results and Discussion The relationship between melting point and molecular weight for the fractions from samples D-4 and K-I is shown in Fig.

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